Navegar

Colección

Datos Estadísticas

Parte de libro

Jiménez, Y.; Otero, M.; Arnau, A. "QCM data analysis and interpretation" (2008) Piezoelectric Transducers and Applications:331-398
La versión final de este artículo es de uso interno de la institución.
Consulte el artículo en la página del editor

Abstract:

The bulk acoustic wave-thickness shear mode resonator (BAW-TSM), whose major representative is the AT-cut quartz crystal, has been introduced in Chap. 1 as a microbalance sensor (QCM). In chapter 3, the basic concepts of modeling were introduced making the use of the resonator evident as a sensor device. Figure 3.1 showed the general schema of a quartz crystal resonator with a multilayer coating, which can be reduced to that of Fig. 14.1 by modeling a 3-layer compound resonator formed by the quartz crystal in contact with a finite viscoelastic layer contacting a semi-infinite viscoelastic medium. This reduced model is appropriate for representing a large number of applications. Changes in the physical properties of the coating are transferred to the electrical admittance or impedance of the resonator, through the acoustic load impedance ZLM (see Chap. 3 and Appendix 3.A), thus allowing its use as a sensor device. Some typical applications of this acoustic wave sensor are the detection of special chemical species, the monitoring of electrochemical processes or the detection of biological molecules (see Chaps. 9, 10, 11, 12 and 13). In chapter 5, the three main steps involved in a TSM resonator sensor were introduced: 1) measurement of the appropriate experimental parameter values for a convenient representation of the resonant response of the sensor, including suitable electronic and cell interfaces (see Chap. 5); 2) extraction of the effective parameter values of the physical model used for representing the resonator sensor (2, 3 or n-layer model-see Chap. 3), and 3) final interpretation of the physical, chemical or biological phenomena responsible for the change in the effective equivalent parameters of the selected physical model. The final interpretation indicated in the third point depends on the application, but it must be coherent with the changes in the effective physicalproperties of the coating, which have been used to define the physical model of the sensor. Thus, previously to the final interpretation of the physical, biological or chemical phenomena, it is necessary the extraction of the physical properties used in the definition of the model starting from the changes in the electrical experimental parameters measured; next, an adequate interpretation of the changes in those properties must be done. This process will be called data analysis. After the data analysis, the final interpretation of the physical, chemical or biological phenomena can be accomplished starting from the changes in the effective physical properties extracted in the data analysis. In many applications, the data analysis is a complex task and, in consequence, the final interpretation is difficult as well. This chapter attempts to clarify this aspect, and for that a set of different cases (from the simplest one to the most complex) will be presented in Sects. 14.3 and 14.4. In each case the data analysis will be described. Next, in Sect. 14.5 some typical applications of the sensor will be introduced as examples for the explanation of the final interpretation of the physical, biological or chemical phenomena. Before that, in Sect. 14.2, the general extraction procedure of the effective physical properties of the coating starting from the electrical parameters measured experimentally will be described. © Springer-Verlag Berlin Heidelberg 2008.

Registro:

Documento: Parte de libro
Título:QCM data analysis and interpretation
Autor:Jiménez, Y.; Otero, M.; Arnau, A.
Filiación:Departamento de Ingeniería Electrónica, Universidad Politécnica de Valencia, Valencia, Spain
Departamento de Física Aplicada, Facultad de Ciencias Exactas y Naturales, Universidad de Buenos Aires /CONICET, Buenos Aires, Argentina
Año:2008
Página de inicio:331
Página de fin:398
DOI: http://dx.doi.org/10.1007/978-3-540-77508-9_14
Título revista:Piezoelectric Transducers and Applications
Título revista abreviado:Piezoelectric Transducers and Applic.
Registro:https://bibliotecadigital.exactas.uba.ar/collection/paper/document/paper_97835407_v_n_p331_Jimenez

Referencias:

  • Hillman, A.R., Jackson, A., Martin, S.J., The problem of uniqueness of fit for viscoelastic films on thickness-shear mode resonator surfaces (2001) Analytical Chemistry, 73 (3), pp. 540-549
  • Behling, C., Lucklum, R., Hauptmann, P., Possibilities and limitations in quantitative determination of polymer shear parameters by tsm resonators (1997) Sensors and Actuators A, 61, pp. 260-266
  • Calvo, E.J., Etchenique, R., Barlett, P.N., Singhal, K., Santamaria, C., Quartz crystal impedance studies at 10mhz of viscoelastic liquids and films (1997) Faraday Discuss, 107, pp. 141-157
  • Bandey, H.L., Hillmann, A.R., Brown, M.J., Martin, S.J., Viscoelastic characterization of electroactive polymer films at electrode/solution interface (1997) Faraday Discuss, 107, pp. 105-121
  • Lucklum, R., Hauptmann, P., Determination of polymer shear modulus with quartz crystal resonators (1997) Faraday Discuss, 107, pp. 123-140
  • Etchenique, R., Dan Weisz, A., Simultaneous determination of mechanical moduli and mass of thin layers using non-Additive quartz crystal acoustic impedance analysis (1999) Journal of Applied Physics, 86 (4), pp. 1994-2000
  • Bund, A., Schneider, M., Characterization of the viscoelasticity an the surface roughness of electrochemically prepared conducting polymer films by impedance measurements at quartz crystals (2002) Journal of Electrochemical Society, 149 (9), pp. 331-339
  • Wolff, O., Seydel, E., Johannsmann, D., Viscoelastic properties of thin films studied with quartz crystal resonators (1997) Faraday Discuss, 107, pp. 91-104
  • Domack, A., Prucker, O., Rühe, J., Johannsmann, D., Swelling of a polymer brush probed with a quartz crystal resonator (1997) The American physical society, 56 (1), pp. 680-689
  • Johannsmann, D., Mathauer, K., Wegner, G., Knoll, W., Viscoelastic properties of thin films probed with a quartz crystal resonator (1992) Physical Review B, 46 (12), pp. 7808-7815
  • Jiménez, Y., Sogorb, T., Arnau, A., Otero, M., Calvo, E.J., Systematic error analysis in the determination of physical parameters of the coating in quartz crystal resonators sensors (2003) AWSWS IV, , Salbris, Francia
  • Granstaff, V.E., Martin, S.J., Characterization of a thickness mode quartz resonator with multiple nonpiezoelectric layers (1994) Journal of Applied Physics, 75 (3), pp. 1319-1329
  • Schröder, J., Borngräber, R., Eichelbaum, F., Hauptmann, P., Advanced interface electronics and methods for qcm (2002) Sensors and actuators A, 97-98, pp. 543-547
  • Arnau, A., Sogorb, T., Jiménez, Y., Thickness-shear mode quartz crystal resonators in viscoelastic fluid media (2000) Journal of Applied Physics, 88 (8), pp. 4498-4506
  • Arnau, A., Jiménez, Y., Sogorb, T., An extended butterworth-van dyke model for quartz crystal microbalance applications in viscoelastic fluid media (2001) IEEE Transactions on Ultrasonics, Ferroelectrics and Frequency Control, 48 (5), pp. 1367-1382
  • Bund, A., Schwitzgebel, G., Viscoelastic properties of low-viscosity liquids studied with thickness-shear mode resonators (1998) Analytical Chemistry, 70, pp. 2584-2588
  • Kankare, J., Sauerbrey equation of quartz crystal microbalance in liquid medium (2002) Langmuir, 18, pp. 7092-7094
  • Voinova, M.V., Jonson, M., Kasemo, B., Missing mass effect in biosensor's qcm applications (2002) Biosensors and Bioelectronics, 17, pp. 835-841
  • Lucklum, R., Behling, C., Hauptmann, P., Role of mass accumulation and viscoelastic film properties for the response of acousticwave-based chemical sensors (1999) Analytical Chemistry, 71 (13), pp. 2488-2496
  • Lucklum, R., Behling, C., Hauptmann, P., Cernosek, R.W., Martin, S.J., Error analysis of material parameter determination with quartz-crystal resonators (1998) Sensors and Actuators A, 66, pp. 184-192
  • Behling, C., Lucklum, R., Hauptmann, P., Fast three-step method for shear moduli calculation from quartz crystal resonator measurements (1999) IEEE Transactions on Ultrasonics Ferroelectrics and Frequency Control, 46 (6), pp. 1431-1438
  • Cernosek, R.W., Martin, S.J., Hillman, A.R., Bandey, H.L., Comparison of lumped-element and transmision-line models for thicknessshear-mode quartz resonator sensors (1998) IEEE Transactions on Ultrasonics, Ferroelectrics and Frequency Control, 45 (5), pp. 1399-1407
  • Azzam, R.M.A., Bashara, N.H., (1997) Ellipsometry and Polarized Light, , North-Holland, Amsterdam
  • Arwin, H., Ellipsometry on thin organic layers of biological interest: Characterization and applications (2000) Thin Solid Films, 48, pp. 377-378
  • Calvo, E.J., Forzani, E., Otero, M., Study of layer-by-layer selfassembled viscoelastic films on thickness-shear mode resonator surfaces (2002) Analytical Chemistry, 74, pp. 3281-3289
  • Lee, S.W., Hinsberg, D., Kanazawa, K., Determination of the viscoelastic properties of polymer films using a compensated phase-locked oscillator circuit (2002) Analytical Chemistry, 74, pp. 125-131
  • Höök, F., Vörös, J., Rodahl, M., Kurrat, R., Böni, P., Ramsden, J.J., Textor, M., Kasemo, B., A comparative study of protein adsorption on titanium oxide surfaces using in situ ellipsometry, optical waveguide light-mode spectroscopy, and quartz crystal microbalance/dissipation (2002) Colloids and Surfaces B: Biointerfaces, 24, pp. 155-179
  • Otero, M., (2003) Construcción y caracterización de estructuras complejas de biomoléculas con aplicación en el diseño de biosensores, , Tesis Doctoral, Universidad de Buenos Aires
  • Ferrante, F., Kipling, A.L., Thompson, M., Molecular slip at the solid-liquid interface o fan acoustic wave sensor (1994) Journal of Applied Physics, 76 (6), pp. 3448-3462
  • Jiménez, Y., (2004) Contribución a la resolución de la problemática asociada a la medida de las propiedades físicas de recubrimientos viscoelásticos en sensores de cuarzo, , Tesis Doctoral, Universidad Politécnica de Valencia
  • Jiménez, Y., Fernández, R., Torres, R., Arnau, A., A contribution o solve the problem of coating properties extraction in quartz crystal microbalance applications (2006) IEEE Transactions on Ultrasonics, Ferroelectrics and Frequency Control, 53 (5), pp. 1057-1072
  • Neto, D., Evans, D., Craig, V., Boundary slip in newtonian liquids: A review of experimental studies (2005) Reports on Progress in Physics, 68, pp. 2859-2897
  • Martin, S.J., Frye, G.C., Ricco, A.J., Senturia, S.D., Effect of surface roughness on the response of thickness-shear mode resonators in liquids (1993) Analytical Chemistry, 65 (20), pp. 2910-2922
  • Schumacher, R., Borges, G., Kanazawa, K.K., The quartz microbalance: A sensitive tool to probe surface reconstructions on gold electrodes in liquid (1985) Surface Science, 163, p. 621
  • Urbakh, M., Daikhin, L., Roughness effect on the frequency of a quartz-crystal resonator in contact with a liquid (1994) Physical Review B, 49 (7), pp. 1866-1870
  • Urbakh, M., Daikhin, L., Influence of the surface morphology on the quartz crystal (1994) Langmuir, 10, pp. 2836-2841
  • Daikhin, L., Urbakh, M., Effect of surface film structure on the quartz crystal microbalance response in liquids (1996) Langmuir, 12, pp. 6354-6360
  • Daikhin, L., Urbakh, M., Influence of surface roughness on the quartz crystal microbalance response in a solution (1997) Faraday Discuss, 107, pp. 27-38
  • Urbakh, M., Daikhin, L., Surface morphology and the quartz crystal microbalancen response in liquids (1998) Colloids and Surfaces A, 134, pp. 75-84
  • Daikhin, L., Gileadi, E., Katz, G., Tsionsky, V., Urbakh, M., Zagidulin, D., Influence of roughness on the admittance of the quartz crystal microbalance immersed in liquids (2002) Analytical Chemistry, 74, pp. 554-561
  • Etchenique, R., Brudny, V.L., Characterization of porous thin films using quartz crystal shear resonators (2000) Langmuir, 16, pp. 5064-5071
  • Wondraczek, K., Bund, A., Johannsmann, D., Acoustic second harmonic generation from rough surfaces under shear excitation in liquids (2004) Langmuir, 20 (23), pp. 10346-10350
  • Wehner, S., Wondraczek, K., Johannsmann, D., Bund, A., Roughness-induced acoustic second-harmonic generation during electrochemical metal deposition on the quartz crystal microbalance (2004) Langmuir, 20 (6), pp. 2356-2360
  • Bund, A., Application of the quartz crystal microbalance for the investigation of nanotribological processes (2004) Journal of Solid State Electrochemistry, 8, pp. 182-186
  • Wondraczek, K., Bund, A., Johannsmann, D., Acoustic second harmonic generation from rough surfaces under shear excitation in liquids (2004) Langmuir, 20 (23), pp. 10346-10350
  • Arnau, A., Jiménez, Y., Fernández, R., Torres, R., Otero, M., Calvo, E.J., Viscoelastic characterization of electrochemically prepared conducting polymer films by impedance analysis at quartz crystal. Study of the surface roughness effect on the effective values of the viscoelastic properties of the coating (2006) Journal of Electrochemical Society, 153 (7), pp. 455-466
  • Brickman, H.C., A calculation of the viscous force exerted by a flowing fluid on a dense swarm of particles (1947) Applied Scientific Research., A1, pp. 27-34
  • Arnau, A., Jiménez, Y., Fernández, R., A new roughness physical model for describing the mechanical impedance of a coated shear resonator immersed in liquids (2005) Acoustic Wave Sensors Workshop V, , Physikzentrum Bad Honnef, Germany
  • Ochoa, L., Jimenez, Y., Arnau, A., Estudio y modelado de la contribución que tiene la rugosidad superficial del sensor o del recubrimiento, sobre la respuesta del cristal de cuarzo como sensor microgravimétrico en fluidos viscosos (2004) Electro, 2004 (26), pp. 139-144
  • Konash, P.L., Bastiaans, G.J., Piezoelectric crystals as detectors for liquid chromatography (1929) Analytical Chemistry, 52, p. 1980
  • Bizet, K., Gabrielli, C., Perrot, H., Immunodetection by quartz crystal microbalance. A new approach for direct detections of rabbit igg and peroxidasa (2000) Applied Biochemistry and Biotechnology, 89, pp. 139-149
  • Mueller, R.M., White, W., Direct gravimetric calibration of a quartz crystal microbalance (1968) Review of Scientific Instruments, 39, pp. 291-295
  • Ullevig, D.M., Evans, J.F., Measurement of sputtering yields and ion beam damage to organic thin films with the quartz crystal microbalance (1980) Analytical Chemistry, 52 (9), pp. 1467-1473
  • Mecca, V.M., A new method of measuring the mass sensitive area of quartz crystal resonators (1989) Journal of Physics E, (22), pp. 59-61
  • Martin, B.A., Hager, H.E., Flow profile above a quartz crystal vibrating in liquid (1989) Journal of Applied Physics, 65 (7), pp. 2627-2629
  • Gabrielli, C., Keddam, M., Torresi, R., Calibration of the electrochemical quartz crystal microbalance (1991) Jounal of Electrochemical Society, 138 (9), pp. 2657-2660
  • Sauerbrey, G., Verwendung von schwingquarzen zur wägung dünner schichten und zur mikrowägung (1959) Zeitschrift Fuer Physik, 155, pp. 206-222
  • Sauerbrey, G., Messung von plattenschwingungen sehr kleiner amplitude durch lichtstrommodulation (1964) Zeitschrift Fuer Physik, 178, pp. 457-471
  • Tenan, M.A., Soares, D.M., Bertran, C.A., Aqueous sol-gel process in the silica-metasilicate system. A microrheological study (2000) Langmuir, 16, pp. 9970-9976
  • Tursiloadi, S., Imai, H., Hirashima, H., Crystallization and sintering behavior of pzt prepared from metal alkoxides" journal of the (1995) Ceramic Society of Japan, 103 (1202), pp. 1069-1072
  • Vercauteren, S., Keizer, K., Vansant, E.F., Luyten, J., Leysen, R., Porous ceramic membranes: Preparation, transport properties and applications (1998) Journal of Porous Materials, 5, pp. 241-258
  • Senguttuvan, G., Settu, T., Kuppusamy, P., Kamaraj, V., Sol-gel synthesis and thermal evaluation of cordierite-zirconia composites (ce-zro2, y-ce-zro2)" j. Mater.synth (1999) Process, 7 (3), pp. 175-185
  • Barrera-Solano, C., Esquivias, L., Messing, G.L., Effect of preparation conditions on phase formation , densification, and microstructure evolution in la-β-Al2-o3/al2o3 composites (1999) Journal of the American Ceramic Society, 82 (5), pp. 1318-1324
  • Muñoz-Aguado, M.J., Gregorkiewitz, M., Sol-gel synthesis of microporous amorphous silica from purely inorganic precursors (1997) Journal of Colloid and Interface Science, 185 (2), pp. 459-465
  • Meixner, D.L., Dyer, P.N., Influence of sol-gel synthesis parameters on the microstructure of particulate silica xerogels (1999) Journal of Sol-Gel Science and Technology, 14 (3), pp. 223-232
  • Santos, L.R.B., Santilli, C.V., Pulcinelli, S.H., Sol-gel transition in sno2 colloidal suspensions: Viscoelastic properties" journal of (1999) Non-Crystaline Solids, 247, pp. 153-157
  • Paulsson, M., Hagerstrom, H., Edsman, K., Rheological studies of the gelation of the acetylated gellan gum (gelrite®) in physiological conditions (1999) European Journal of Pharmaceutical Science, 9 (1), pp. 99-105
  • Chiu, H.T., Wang, J.H., A study of rheological behavior of a polypyrrole modified uhmwpe gel using a parallel plate rheometer (1999) Polymer Engineering and Science, 39 (9), pp. 1769-1775
  • Puyol, P., Cotter, P.F., Mulvihill, D.M., Thermal gelation of commercial whey protein concentrate: Influence of ph 4.6 insoluble protein on thermal gelation (1999) International Journal of Dairy Technology, 52 (3), pp. 81-91
  • Iler, R.K., (1979) The Chemistry of silica, 173. , Wiley, New York
  • Brinker, C.J., Scherer, G.W., (1990) Sol-Gel SciencesThe Physicsand Chemistry of Sol-Gel Processing, p. 100. , Academic Press, Boston
  • Arias, A.C., Granström, M., Thomas, D.S., Petritsh, K., Friend, R.H., Doped conducting-polymer-semiconducting-polymer interfaces: Their use in organic photovoltaic devices (1999) Physical Review, 60, pp. 1854-1860
  • Piro, B., Dang, L.A., Pham, M.C., Fabiano, S., Tran-Minh, C., A glucose biosensor based on modified-enzyme incorporated within electropolymerised poly(3,4-ethylenedioxythiophene) (pedt) films (2001) Journal of Electroanalytical Chemistry, 512, pp. 101-109
  • Goenendaal, L., Jonas, F., Freitag, D., Pielartzik, H., Rynolds, J.R., Poly(3,4-ethylenedioxythiophene) and its derivatives: Past, present, and future (2000) Advanced Materials, 12 (7), pp. 481-494
  • Rammelt, U., Nguyen, P.T., Plieth, W., Protection of mild steel by modification with thin films of polymethylthiophene (2001) Electrochimica Acta, 46, pp. 4251-4257
  • Pagés, H., Topart, P., Lemordant, D., Wide band electrochromic displays based on thin conducting polymer films (2001) Electrochimica Acta, 46, pp. 2137-2143
  • Randriamakazaka, H., Noel, V., Chevrot, C., Nucleation and growth of poly(3,4-ethylenedioxythiophene) in acetonitrile on platinum under potentiostatic conditions (1999) Journal of Electroanalytical Chemistry, 472 (2), pp. 103-111
  • Johannsmann, D., Grunner, J., Wesser, J., Mathauer, K., Wegner, G., Knoll, W., Viscoelastic properties of thin-films probed with a quartz crystal resonator (1992) Thin Solid Films, 210, pp. 662-665
  • Calvo, E.J., Danilowitz, C., Forzani, E., Wolosiuk, A., Otero, M., Biomolecular films: Design, function and applications (2003) J. Rusling (Ed), 337p. , Marcel Dekker
  • Höok, F., Kasemo, B., Nylander, T., Fant, C., Scott, K., Elwing, H., Variations in coupled water, viscoelastic properties, and film thickness of a mefp-1 protein film during adsorption and cross-linking: A quartz crystal microbalance with dissipation monitoring, ellipsometry, and surface plasmon resonance study (2001) Analytical Chemistry, 73, pp. 5796-5804

Citas:

---------- APA ----------
Jiménez, Y., Otero, M. & Arnau, A. (2008) . QCM data analysis and interpretation. Piezoelectric Transducers and Applications, 331-398.
http://dx.doi.org/10.1007/978-3-540-77508-9_14
---------- CHICAGO ----------
Jiménez, Y., Otero, M., Arnau, A. "QCM data analysis and interpretation" . Piezoelectric Transducers and Applications (2008) : 331-398.
http://dx.doi.org/10.1007/978-3-540-77508-9_14
---------- MLA ----------
Jiménez, Y., Otero, M., Arnau, A. "QCM data analysis and interpretation" . Piezoelectric Transducers and Applications, 2008, pp. 331-398.
http://dx.doi.org/10.1007/978-3-540-77508-9_14
---------- VANCOUVER ----------
Jiménez, Y., Otero, M., Arnau, A. QCM data analysis and interpretation. Piezoelectric Transducers and Applic. 2008:331-398.
http://dx.doi.org/10.1007/978-3-540-77508-9_14