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Abstract:

TiO 2 thin films deposited by a vacuum arc on a glass substrate were characterized by X-ray reflectivity (XRR), X-ray diffraction (XRD), scanning electron microscopy (SEM) and atomic force microscopy (AFM). Several thin films with different amounts of deposited TiO 2 mass and different deposition and annealing temperatures were studied. A qualitative analysis of the XRD patterns indicated the presence of the anatase and/or rutile crystalline phases in most of the studied samples. From the analysis of the experimental XRR curves - which exhibited a wide angular range of oscillatory behavior - the thickness, mass density and interface roughness were determined. All XRR patterns were well fitted by modeled curves that assume the presence of a single and homogeneous TiO 2 layer over which a very thin H 2 O layer is adsorbed. The thickest H 2 O adsorption layers were developed in films with the highest anatase content. Our overall results of the XRR analyses are consistent with those derived from the imaging techniques (SEM and AFM). Copyright © 2014 American Scientific Publishers.

Registro:

Documento: Artículo
Título:X-ray reflectivity analysis of titanium dioxide thin films grown by cathodic arc deposition
Autor:Kleiman, A.; Lamas, D.G.; Craievich, A.F.; Márquez, A.
Filiación:Consejo Nacional de Investigaciones Científicas y Técnicas (CONICET), Av. Rivadavia 1917, C1033AAJ Buenos Aires, Argentina
Instituto de Física Del Plasma (INFIP), Departamento de Física, Universidad de Buenos Aires, Ciudad Universitaria, Pabellón I, C1428EHA Buenos Aires, Argentina
Facultad de Ingeniería, Laboratorio de Caracterización de Materiales, Universidad Nacional Del Comahue, Buenos Aires 1400, Q8300IBX Neuquén, Argentina
Instituto de Física, Universidade de São Paulo, Cidade Universitaria, Travessa R da Rua do Matao, No. 187, 05508-900 São Paulo, Brazil
Palabras clave:Cathodic Arc Deposition; Thin Films; X-Ray Reflectivity; Atomic force microscopy; Imaging techniques; Oxide minerals; Scanning electron microscopy; Substrates; Thin films; Titanium dioxide; Vacuum applications; X ray diffraction; Annealing temperatures; Cathodic arc deposition; Oscillatory behaviors; Qualitative analysis; TiO; Titanium dioxide thin film; X ray reflectivity; X-ray reflectivity analysis; Deposition
Año:2014
Volumen:14
Número:5
Página de inicio:3902
Página de fin:3909
DOI: http://dx.doi.org/10.1166/jnn.2014.8017
Título revista:Journal of Nanoscience and Nanotechnology
Título revista abreviado:J. Nanosci. Nanotechnol.
ISSN:15334880
CODEN:JNNOA
Registro:https://bibliotecadigital.exactas.uba.ar/collection/paper/document/paper_15334880_v14_n5_p3902_Kleiman

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Citas:

---------- APA ----------
Kleiman, A., Lamas, D.G., Craievich, A.F. & Márquez, A. (2014) . X-ray reflectivity analysis of titanium dioxide thin films grown by cathodic arc deposition. Journal of Nanoscience and Nanotechnology, 14(5), 3902-3909.
http://dx.doi.org/10.1166/jnn.2014.8017
---------- CHICAGO ----------
Kleiman, A., Lamas, D.G., Craievich, A.F., Márquez, A. "X-ray reflectivity analysis of titanium dioxide thin films grown by cathodic arc deposition" . Journal of Nanoscience and Nanotechnology 14, no. 5 (2014) : 3902-3909.
http://dx.doi.org/10.1166/jnn.2014.8017
---------- MLA ----------
Kleiman, A., Lamas, D.G., Craievich, A.F., Márquez, A. "X-ray reflectivity analysis of titanium dioxide thin films grown by cathodic arc deposition" . Journal of Nanoscience and Nanotechnology, vol. 14, no. 5, 2014, pp. 3902-3909.
http://dx.doi.org/10.1166/jnn.2014.8017
---------- VANCOUVER ----------
Kleiman, A., Lamas, D.G., Craievich, A.F., Márquez, A. X-ray reflectivity analysis of titanium dioxide thin films grown by cathodic arc deposition. J. Nanosci. Nanotechnol. 2014;14(5):3902-3909.
http://dx.doi.org/10.1166/jnn.2014.8017