Artículo
Giudicessi, S.L.; Fatema, M.K.; Nonami, H.; Erra-Balsells, R. "Ethylenediaminetetraacetic acid (EDTA) as an auxiliary tool in the electrospray ionization mass spectrometry analysis of native and derivatized β-cyclodextrins, maltoses, and fructans contaminated with Ca and/or Mg" (2010) Journal of the American Society for Mass Spectrometry. 21(9):1526-1529
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Abstract:
The effect of Ca2+ (and Mg2+) and the disodium salt of ethylenediaminetetraacetic acid (EDTA), a well known Ca2+ (and Mg2+) chelating agent, on the volatilization/ionization of carbohydrates by using electrospray ionization mass spectrometry has been studied. Model compounds such as maltoses (maltose to maltoheptaose), β-cyclodextrins (β-cyclodextrin, methyl-β-cyclodextrin, heptakis(2,6-di-O-methyl)-β-cyclodextrin, heptakis(2,3,6-tri-O-methyl)-β-cyclodextrin, and 2-hydroxypropyl-β-cyclodextrin) and fructans (sucrose, 1-ketose, nystose, and 1F-fructofuranosylnystose) were used. © 2010.
Registro:
| Documento: | Artículo |
| Título: | Ethylenediaminetetraacetic acid (EDTA) as an auxiliary tool in the electrospray ionization mass spectrometry analysis of native and derivatized β-cyclodextrins, maltoses, and fructans contaminated with Ca and/or Mg |
| Autor: | Giudicessi, S.L.; Fatema, M.K.; Nonami, H.; Erra-Balsells, R. |
| Filiación: | CIHIDECAR-CONICET, Departamento de Química Orgánica, Facultad de Ciencias Exactas y Naturales, Universidad de Buenos Aires, Buenos Aires, Argentina Plant Biophysics/Biochem. Research Laboratory, Faculty of Agriculture, Ehime University, Matsuyama, Japan |
| Palabras clave: | Chelating agent; Disodium salt; Electrospray ionization mass spectrometry; Ethylenediaminetetraacetic acid; Fructans; Maltoheptaose; Model compound; Acids; Calcium; Carbohydrates; Chelation; Cyclodextrins; Electrospray ionization; Ionization; Maltose; Mass spectrometry; Particle detectors; Polysaccharides; Sugar (sucrose); Silanes; 1 ketose; 1f fructofuramosylnystose; 2 hydroxypropyl beta cyclodextrin; beta cyclodextrin; beta cyclodextrin derivative; beta cyclodextrin methyl ester; calcium ion; edetic acid; enzyme; fructan; heptakis(2,3,6 o trimethyl) beta cyclodextrin; heptakis(2,6 o dimethyl) beta cyclodextrin; magnesium ion; maltoheptaose; maltose; nystose; sucrose; unclassified drug; article; carbohydrate analysis; chemical analysis; controlled study; electrospray mass spectrometry; ionization; volatilization; beta-Cyclodextrins; Calcium; Edetic Acid; Fructans; Magnesium; Maltose; Spectrometry, Mass, Electrospray Ionization |
| Año: | 2010 |
| Volumen: | 21 |
| Número: | 9 |
| Página de inicio: | 1526 |
| Página de fin: | 1529 |
| DOI: | http://dx.doi.org/10.1016/j.jasms.2010.05.002 |
| Título revista: | Journal of the American Society for Mass Spectrometry |
| Título revista abreviado: | J. Am. Soc. Mass Spectrom. |
| ISSN: | 10440305 |
| CODEN: | JAMSE |
| CAS: | 2 hydroxypropyl beta cyclodextrin, 94035-02-6; beta cyclodextrin, 7585-39-9; calcium ion, 14127-61-8; edetic acid, 150-43-6, 60-00-4; fructan, 9037-90-5; heptakis(2,6 o dimethyl) beta cyclodextrin, 51166-71-3; magnesium ion, 22537-22-0; maltoheptaose, 1980-14-9, 34620-78-5; maltose, 16984-36-4, 69-79-4; sucrose, 122880-25-5, 57-50-1; Calcium, 7440-70-2; Edetic Acid, 60-00-4; Fructans; Magnesium, 7439-95-4; Maltose, 69-79-4; beta-Cyclodextrins |
| PDF: | https://bibliotecadigital.exactas.uba.ar/download/paper/paper_10440305_v21_n9_p1526_Giudicessi.pdf |
| Registro: | https://bibliotecadigital.exactas.uba.ar/collection/paper/document/paper_10440305_v21_n9_p1526_Giudicessi |
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Citas:
---------- APA ----------
Giudicessi, S.L., Fatema, M.K., Nonami, H. & Erra-Balsells, R. (2010) . Ethylenediaminetetraacetic acid (EDTA) as an auxiliary tool in the electrospray ionization mass spectrometry analysis of native and derivatized β-cyclodextrins, maltoses, and fructans contaminated with Ca and/or Mg. Journal of the American Society for Mass Spectrometry, 21(9), 1526-1529.http://dx.doi.org/10.1016/j.jasms.2010.05.002
---------- CHICAGO ----------
Giudicessi, S.L., Fatema, M.K., Nonami, H., Erra-Balsells, R. "Ethylenediaminetetraacetic acid (EDTA) as an auxiliary tool in the electrospray ionization mass spectrometry analysis of native and derivatized β-cyclodextrins, maltoses, and fructans contaminated with Ca and/or Mg" . Journal of the American Society for Mass Spectrometry 21, no. 9 (2010) : 1526-1529.http://dx.doi.org/10.1016/j.jasms.2010.05.002
---------- MLA ----------
Giudicessi, S.L., Fatema, M.K., Nonami, H., Erra-Balsells, R. "Ethylenediaminetetraacetic acid (EDTA) as an auxiliary tool in the electrospray ionization mass spectrometry analysis of native and derivatized β-cyclodextrins, maltoses, and fructans contaminated with Ca and/or Mg" . Journal of the American Society for Mass Spectrometry, vol. 21, no. 9, 2010, pp. 1526-1529.http://dx.doi.org/10.1016/j.jasms.2010.05.002
---------- VANCOUVER ----------
Giudicessi, S.L., Fatema, M.K., Nonami, H., Erra-Balsells, R. Ethylenediaminetetraacetic acid (EDTA) as an auxiliary tool in the electrospray ionization mass spectrometry analysis of native and derivatized β-cyclodextrins, maltoses, and fructans contaminated with Ca and/or Mg. J. Am. Soc. Mass Spectrom. 2010;21(9):1526-1529.http://dx.doi.org/10.1016/j.jasms.2010.05.002
