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Abstract:

The 13C NMR spectra 17 derivatives of androst-4-ene-3,17-dione were recorded and assigned. Assignments were based on spectral comparison with compounds of similar structure and distortionless enhancement by polarization transfer (DEPT) NMR measurements.

Registro:

Documento: Artículo
Título:Cyclothioacetals and cycloacetals of androst-4-ene-3,17-dione and related compounds. 13C NMR spectral assignments
Autor:Caballero, G.M.; Gros, E.G.
Filiación:Depto. de Quimca Organica, Universidad de Buenos Aires, Ciudad Universitaria, 1428 Buenos Aires, Argentina
Palabras clave:13C NMR; Androst-4-ene-3, 17-dione; Cycloacetals; Cyclothioacetals; DEPT; NMR
Año:1996
Volumen:34
Número:2
Página de inicio:162
Página de fin:164
DOI: http://dx.doi.org/10.1002/(SICI)1097-458X(199602)34:2<162::AID-OMR834>3.0.CO;2-U
Título revista:Magnetic Resonance in Chemistry
Título revista abreviado:Magn. Reson. Chem.
ISSN:07491581
CODEN:MRCHE
Registro:https://bibliotecadigital.exactas.uba.ar/collection/paper/document/paper_07491581_v34_n2_p162_Caballero

Referencias:

  • Caballero, G.M., Gros, E.G., (1989) J. Chem. Res. (S), p. 320
  • Caballero, G.M., Gros, E.G., (1995) Synth. Commun., 25, p. 395
  • Caballero, G.M., Gros, E.G., (1991) J. Labelled Compd. Radiopharm., 29, p. 805
  • Caballero, G.M., Gros, E.G., (1993) J. Labelled Compd. Radiopharm., 33, p. 907
  • Caballero, G.M., Gros, E.G., (1994) J. Labelled Compd. Radiopharm., 34, p. 127
  • Doddrell, D.M., Pegg, D.T., Bendall, M.R., (1982) J. Magn. Reson., 48, p. 323
  • Williams, J.R., Sarkisian, G.M., (1974) Synthesis, p. 32
  • Weiss, R.G., Snyder, E.I., (1971) J. Org. Chem., 36, p. 403
  • Blunt, J.W., Stothers, J.B., (1977) Org. Magn. Reson., 9, p. 439

Citas:

---------- APA ----------
Caballero, G.M. & Gros, E.G. (1996) . Cyclothioacetals and cycloacetals of androst-4-ene-3,17-dione and related compounds. 13C NMR spectral assignments. Magnetic Resonance in Chemistry, 34(2), 162-164.
http://dx.doi.org/10.1002/(SICI)1097-458X(199602)34:2<162::AID-OMR834>3.0.CO;2-U
---------- CHICAGO ----------
Caballero, G.M., Gros, E.G. "Cyclothioacetals and cycloacetals of androst-4-ene-3,17-dione and related compounds. 13C NMR spectral assignments" . Magnetic Resonance in Chemistry 34, no. 2 (1996) : 162-164.
http://dx.doi.org/10.1002/(SICI)1097-458X(199602)34:2<162::AID-OMR834>3.0.CO;2-U
---------- MLA ----------
Caballero, G.M., Gros, E.G. "Cyclothioacetals and cycloacetals of androst-4-ene-3,17-dione and related compounds. 13C NMR spectral assignments" . Magnetic Resonance in Chemistry, vol. 34, no. 2, 1996, pp. 162-164.
http://dx.doi.org/10.1002/(SICI)1097-458X(199602)34:2<162::AID-OMR834>3.0.CO;2-U
---------- VANCOUVER ----------
Caballero, G.M., Gros, E.G. Cyclothioacetals and cycloacetals of androst-4-ene-3,17-dione and related compounds. 13C NMR spectral assignments. Magn. Reson. Chem. 1996;34(2):162-164.
http://dx.doi.org/10.1002/(SICI)1097-458X(199602)34:2<162::AID-OMR834>3.0.CO;2-U