Navegar

Colección

Datos Estadísticas

Artículo

Estamos trabajando para incorporar este artículo al repositorio
Consulte el artículo en la página del editor
Consulte la política de Acceso Abierto del editor

Abstract:

In contrast with the spectra previously measured with lower resolution equipment, the 500-MHz 1H NMR spectra of l, l-bis(acetam1do)-1-deoxy-D-gl ucitol peracetate and N-acetyl-α-D-galactopyranosylamine peracetate in aqueous solution were amenable to full resolution. The former compound shows a “sickle” conformation produced by rotation of the C2–C3 bond out of the planar, zigzag arrangement, while the latter has a 4C1conformation. © 1987, Taylor & Francis Group, LLC. All rights reserved.

Registro:

Documento: Artículo
Título:The high-resolution 1h nmr spectra and conformations of n-acetyl-α-d-galactopyranosylamine peracetate and 1, 1-bis(acetamido)-l-deoxy-d-glucitol peracetate in aqueous medium
Autor:Matulewicz, M.C.; Stortz, C.A.; Jarret, R.M.; Cerezo, A.S.
Filiación:Departamento De Quimica Orgánica, Facultad De Ciencias Exactas y Naturales, Ciudad Universitaria, Pabellon 2, 1428, Buenos, A1res, Argentina
College of the Holy Cross, Department of Chemistry, Worcester, MA, 01610, United States
Año:1987
Volumen:6
Número:3
Página de inicio:515
Página de fin:521
DOI: http://dx.doi.org/10.1080/07328308708057939
Título revista:Journal of Carbohydrate Chemistry
Título revista abreviado:J. Carbohydr. Chem.
ISSN:07328303
Registro:https://bibliotecadigital.exactas.uba.ar/collection/paper/document/paper_07328303_v6_n3_p515_Matulewicz

Referencias:

  • Coxon, B., Tipson, R.S., Alexander, M., Deferrari, J.O., (1974) Carbohydr. Res., 35 (15)
  • Wang, L., Lin, T.-S., Sartorelli, A.C., (1983) J. Org. Chem., 48 (2891)
  • Cerezo, A.S., (1971) Chem. Ind., 96
  • Cerezo, A.S., (1978) An. Asoc. Quim. Argent., 66 (41)
  • Seldes, A.M., Gros, E.G., Thiel, I.M.E., Deferrari, J.O., (1975) Carbohydr. Res., 39 (11)
  • El Khadem, H., Horton, D., Wander, J.D., (1972) J. Org. Chem., 37 (1630)
  • Richardson, A.C., Mclauchlan, K.A., (1962) J. Chem. Soc., 2499. , (in part)
  • Cerezo, A.S., Sproviero, J.F., Deulofeu, V., Delpy, S., (1968) Carbohydr. Res., 7 (395)
  • Frush, H.L., Isbell, H.S., (1951) J. Res. Nat. Bur. Stand., 47 (239)

Citas:

---------- APA ----------
Matulewicz, M.C., Stortz, C.A., Jarret, R.M. & Cerezo, A.S. (1987) . The high-resolution 1h nmr spectra and conformations of n-acetyl-α-d-galactopyranosylamine peracetate and 1, 1-bis(acetamido)-l-deoxy-d-glucitol peracetate in aqueous medium. Journal of Carbohydrate Chemistry, 6(3), 515-521.
http://dx.doi.org/10.1080/07328308708057939
---------- CHICAGO ----------
Matulewicz, M.C., Stortz, C.A., Jarret, R.M., Cerezo, A.S. "The high-resolution 1h nmr spectra and conformations of n-acetyl-α-d-galactopyranosylamine peracetate and 1, 1-bis(acetamido)-l-deoxy-d-glucitol peracetate in aqueous medium" . Journal of Carbohydrate Chemistry 6, no. 3 (1987) : 515-521.
http://dx.doi.org/10.1080/07328308708057939
---------- MLA ----------
Matulewicz, M.C., Stortz, C.A., Jarret, R.M., Cerezo, A.S. "The high-resolution 1h nmr spectra and conformations of n-acetyl-α-d-galactopyranosylamine peracetate and 1, 1-bis(acetamido)-l-deoxy-d-glucitol peracetate in aqueous medium" . Journal of Carbohydrate Chemistry, vol. 6, no. 3, 1987, pp. 515-521.
http://dx.doi.org/10.1080/07328308708057939
---------- VANCOUVER ----------
Matulewicz, M.C., Stortz, C.A., Jarret, R.M., Cerezo, A.S. The high-resolution 1h nmr spectra and conformations of n-acetyl-α-d-galactopyranosylamine peracetate and 1, 1-bis(acetamido)-l-deoxy-d-glucitol peracetate in aqueous medium. J. Carbohydr. Chem. 1987;6(3):515-521.
http://dx.doi.org/10.1080/07328308708057939