Registro:

Referencias:

• Mulvey, R.E., (1991) Chem. Soc. Rev., 20, pp. 167-209. , Review
• Gregory, K., Schleyer, Snaith, R., (1991) Adv. Inorg. Chem., 37, pp. 47-142. , Review
• Gilchrist, J.H., Collum, D.B., (1992) J. Am. Chem. Soc., 114, pp. 794-795
• Hall, P.L., Gilchrist, J.H., Harrison, A.T., Fuller, D.J., Collum, D.B., (1991) J. Am. Chem. Soc., 113. , 9575–9585, and references cited therein
• Wanat, R.A., Collum, D.B., Van Duyne, G., Clardy, J., De Pue, R.T., (1986) J. Am. Chem. Soc., 108, p. 3422. , 3415
• Sato, D., Kawasaki, H., Shimada, I., Arata, Y., Okamura, K., Date, T., Koga, K., (1992) J. Am. Chem. Soc., 114, pp. 761-763
• Jackman, L.M., Scarmoutzos, L.M., Smith, B.D., Williard, P.G., (1988) J. Am. Chem. Soc., 110, pp. 6058-6063
• Nudelman, N.S., (1989) Carbonylation of Main‐Group Organometallic Compounds in The Chemistry of Double‐Bonded Functional Groups, pp. 799-962. , Review:, S. Patai, Wiley, Chichester
• Nudelman, N.S., Lewkowicz, E.S., Pérez, D.G., (1990), Synthesis, 917–920; Pérez, D.G., Nudelman, N.S., (1983) J. Org. Chem., 48, pp. 133-134
• Furlong, J.J.P., Lewkowicz, E.S., Nudelman, N.S., (1990), J. Chem. Soc. Perkin Trans 2, 1461–1465; Nudelman, N.S., Pérez, D.G., (1989), J. Chem. Soc. Perkin Trans 2, 931–936; Rautenstrauch, V., Joyeux, M., (1979) Angew. Chem., 91. , 73–74
• (1979) Angew. Chem. Int. Ed. Engl., 18. , 85
• Pérez, D.G., Nudelman, N.S., (1988) J. Org. Chem., 53, pp. 408-413
• Nudelman, N.S., Lewkowicz, E., Furlong, J.J.P., J. Org. Chem; Barr, D., Clegg, W., Mulvey, R.E., Snaith, R., (1984), J. Chem. Soc. Chem. Commun., 469–470; Clegg, W., MacGregor, M., Mulvey, R.E., O'Neil, P.A., (1992) Angew. Chem., 104, pp. 74-76
• (1992) Angew. Chem. Int. Ed. Engl., 31. , 93
• Crystal data for [1‐Li · 1‐H]4:(C40H84Li4N8), orthorhombic space group Pna21, a = 22.077(1), b = 12.230(1), c = 16.528(1) Å. Data collection with an Enraf‐Nonius CAD4 diffractometer, CuKα radiation, 193 K, 6086 measured reflections, 5578 independent, 4295 observed (F0 > 4σF0). Solution and refinement with the Siemens SHELXTL‐PLUS package (direct methods) [12–14]. One solvent molecule is twofold disordered (0.54:0.46). Disordered positions have been refined with isotropic temperature factors, the other non‐hydrogen atoms anisotropic, hydrogen atoms with common isotropic temperature factors, C‐bonded and disordered N‐bonded H atoms riding, other N‐bonded H atoms have been refined. 477 parameters, R = 0.0606, wR = 0.0491. An absolute structure could not be determined. Further details of the crystal structure investigation may be obtained from the Fachinformationszentrum Karlsruhe, Gesellschaft für wissenschaft‐lich‐technische Information mbH, D‐W‐7514 Eggenstein‐Leopoldshafen 2 (FRG) on quoting the deposition number CSD 320 464, the names of the authors, and the journal citation; SHELXTL‐PLUS (VMS), Release 4.2, Siemens Analytical Instruments, 1991; Spek, A.L., PLATON 88, Program for Geometrical Analysis of Crystal Structures, Utrecht, 1988; Keller, E., SCHAKAL‐88B, A FORTRAN Program for the Graphic Representation of Molecular and Crystallographic Models, Freiburg, 1988; Armstrong, D.R., Barr, D., Clegg, W., Hodgson, S.M., Mulvey, R.E., Reed, D., Snaith, R., Wright, D.S., (1989) J. Am. Chem. Soc., 111, pp. 4719-4727
• Armstrong, D.R., Mulvey, R.E., Walker, G.T., Barr, D., Snaith, R., Clegg, W., Reed, D., (1988), J. Chem. Soc. Dalton Trans., 617–628; Armstrong, D.R., Barr, D., Clegg, W., Mulvey, R.E., Reed, D., Snaith, R., Wade, K., (1986), J. Chem. Soc. Chem. Commun., 869–870; It is probably long lithium amide ladders that precipitate from the solution immediately after the last complexing amine molecules have been lithiated [1, 2]

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