Abstract:
Hybrid materials were developed via in situ oxidative polymerization of aniline in presence of 0.5 wt% of nano-/micro-particles. Polymerization was carried out in hydrochloric acid (HCl) medium. Four types of particles were used (aluminum powder 140 mesh, carbon nanotubes and quartz dust in two sizes, 400 and 140 mesh). Polyaniline and hybrid materials were characterized by spectroscopic techniques (UV-Vis, FT-IR), thermal analyses (TGA, DSC), morphological studies (FE-SEM); electrical conductivity and wear resistance measurements. The most promising hybrids were obtained by the incorporation of aluminum (140 mesh) or quartz 400 mesh powders. In both cases, electrical conductivity was similar to the one measured for PANI but up to 40% higher wear resistance. © 2011 Elsevier B.V. All rights reserved.
Registro:
Documento: |
Artículo
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Título: | Effects of different nucleating particles on aniline polymerization |
Autor: | Lissarrague, M.H.; Lamanna, M.E.; D'Accorso, N.B.; Goyanes, S. |
Filiación: | LP and MC, Departamento de Física, Ciudad Universitaria 1428, Ciudad Autónoma de Buenos Aires, Argentina CIHIDECAR-CONICET, Departamento de Química Orgánica, Ciudad Universitaria 1428, Ciudad Autónoma de Buenos Aires, Argentina
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Palabras clave: | Electrical conductivity; Hybrid materials; PANI; Wear resistance; Aluminum powders; Aniline polymerization; Electrical conductivity; In-situ; Morphological study; PANI; Quartz dust; Resistance measurement; Spectroscopic technique; Aluminum; Aniline; Electric conductivity; Hybrid materials; Hydrochloric acid; Polyaniline; Quartz; Thermoanalysis; Wear resistance; Polymerization |
Año: | 2012
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Volumen: | 162
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Número: | 11-12
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Página de inicio: | 1052
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Página de fin: | 1058
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DOI: |
http://dx.doi.org/10.1016/j.synthmet.2011.12.018 |
Título revista: | Synthetic Metals
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Título revista abreviado: | Synth Met
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ISSN: | 03796779
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CODEN: | SYMED
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Registro: | https://bibliotecadigital.exactas.uba.ar/collection/paper/document/paper_03796779_v162_n11-12_p1052_Lissarrague |
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Citas:
---------- APA ----------
Lissarrague, M.H., Lamanna, M.E., D'Accorso, N.B. & Goyanes, S.
(2012)
. Effects of different nucleating particles on aniline polymerization. Synthetic Metals, 162(11-12), 1052-1058.
http://dx.doi.org/10.1016/j.synthmet.2011.12.018---------- CHICAGO ----------
Lissarrague, M.H., Lamanna, M.E., D'Accorso, N.B., Goyanes, S.
"Effects of different nucleating particles on aniline polymerization"
. Synthetic Metals 162, no. 11-12
(2012) : 1052-1058.
http://dx.doi.org/10.1016/j.synthmet.2011.12.018---------- MLA ----------
Lissarrague, M.H., Lamanna, M.E., D'Accorso, N.B., Goyanes, S.
"Effects of different nucleating particles on aniline polymerization"
. Synthetic Metals, vol. 162, no. 11-12, 2012, pp. 1052-1058.
http://dx.doi.org/10.1016/j.synthmet.2011.12.018---------- VANCOUVER ----------
Lissarrague, M.H., Lamanna, M.E., D'Accorso, N.B., Goyanes, S. Effects of different nucleating particles on aniline polymerization. Synth Met. 2012;162(11-12):1052-1058.
http://dx.doi.org/10.1016/j.synthmet.2011.12.018