Artículo
Caballero, G.M.; Gros, E.G. "Synthesis of [21‐13C]‐cholesterol" (1994) Journal of Labelled Compounds and Radiopharmaceuticals. 34(2):127-130
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Abstract:
The synthesis of [21‐13C]‐cholesterol (5) from 3β‐O‐(t‐butyldimethylsilyl)‐17β‐cyano‐androst‐5‐ene (1) is described. Labelled carbon‐atom was introduced by Grignard reaction of nitrile derivative with [13C]‐methylmagnesium iodide. Location of label was confirmed by 13C‐NMR spectroscopy. Copyright © 1994 John Wiley & Sons, Ltd.
Registro:
| Documento: | Artículo |
| Título: | Synthesis of [21‐13C]‐cholesterol |
| Autor: | Caballero, G.M.; Gros, E.G. |
| Filiación: | Departamento de Quimica Orgánica, Facultad de Ciencias Exactas y Naturales, Universidad de Buenos Aires, Ciudad Universitaria, 1428 Buenos Aires, Buenos Aires, Argentina |
| Palabras clave: | synthesis; [21‐13C]‐cholesterol; carbon 13; cholesterol; article; cholesterol synthesis; controlled study; isotope labeling |
| Año: | 1994 |
| Volumen: | 34 |
| Número: | 2 |
| Página de inicio: | 127 |
| Página de fin: | 130 |
| DOI: | http://dx.doi.org/10.1002/jlcr.2580340204 |
| Título revista: | Journal of Labelled Compounds and Radiopharmaceuticals |
| Título revista abreviado: | J. Label. Compd. Radiopharm. |
| ISSN: | 03624803 |
| Registro: | https://bibliotecadigital.exactas.uba.ar/collection/paper/document/paper_03624803_v34_n2_p127_Caballero |
Referencias:
- Porto, A.M., Gros, E.G., (1971) Experientia, 27, p. 506
- Garraffo, H.M., Gros, E.G., (1986) Steroids, 48, p. 251. , and previous papers cited therein
- Garraffo, H.M., Burton, G., Porto, A.M., Gros, E.G., (1982) An. Asoc. Quim. Argent., 70, p. 743
- Gros, E.G., (1986) Anal. Acad. Nac. Cs. Ex. Fis. Nat., 38, p. 17
- Corey, E.J., Venkateswarlu, A., (1972) J. Am. Chem. Soc., 94, p. 6190
- Schow, S.R., McMorris, T.C., (1979) J. Org. Chem., 44, p. 3760
- DuBois, G.E., (1982) J. Org. Chem., 47, p. 5035
Citas:
---------- APA ----------
Caballero, G.M. & Gros, E.G. (1994) . Synthesis of [21‐13C]‐cholesterol. Journal of Labelled Compounds and Radiopharmaceuticals, 34(2), 127-130.http://dx.doi.org/10.1002/jlcr.2580340204
---------- CHICAGO ----------
Caballero, G.M., Gros, E.G. "Synthesis of [21‐13C]‐cholesterol" . Journal of Labelled Compounds and Radiopharmaceuticals 34, no. 2 (1994) : 127-130.http://dx.doi.org/10.1002/jlcr.2580340204
---------- MLA ----------
Caballero, G.M., Gros, E.G. "Synthesis of [21‐13C]‐cholesterol" . Journal of Labelled Compounds and Radiopharmaceuticals, vol. 34, no. 2, 1994, pp. 127-130.http://dx.doi.org/10.1002/jlcr.2580340204
---------- VANCOUVER ----------
Caballero, G.M., Gros, E.G. Synthesis of [21‐13C]‐cholesterol. J. Label. Compd. Radiopharm. 1994;34(2):127-130.http://dx.doi.org/10.1002/jlcr.2580340204
