Artículo
Doller, D.; Gros, E.G. "Preparation of |2,4‐2H|‐ and |2,4‐3H|‐tomatidine" (1986) Journal of Labelled Compounds and Radiopharmaceuticals. 23(1):109-112
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Abstract:
The preparation of |2,4‐2H|‐ and |2,4‐3H|‐tomatidine was accomplished by oxydation of the unlabelled compound to tomatidone, exchange of the labile hydrogens by reaction with H20 and 3H2O on basic alumina and direct reduction of the labelled tomatidone to tomatidine. The efficiency of the procedure was checked by physical (1H and 13C NMR, MS) methods. Copyright © 1986 John Wiley & Sons, Ltd.
Registro:
| Documento: | Artículo |
| Título: | Preparation of |2,4‐2H|‐ and |2,4‐3H|‐tomatidine |
| Autor: | Doller, D.; Gros, E.G. |
| Filiación: | Departamento de Quimica Orgànica Y Umymfor, Facultad de Ciencias Exactas Y Naturales, Universidad de Buenos Aires, Pabellón 2, Ciudad Universitaria, Buenos Aires, 1428, Argentina |
| Palabras clave: | |2,4‐2H|‐Tomatidine; |2,4‐3H|‐Tomatidine; radioisotope; methodology; nonhuman; priority journal; theoretical study; tomatidine h 2; tomatidine h 3 |
| Año: | 1986 |
| Volumen: | 23 |
| Número: | 1 |
| Página de inicio: | 109 |
| Página de fin: | 112 |
| DOI: | http://dx.doi.org/10.1002/jlcr.2580230114 |
| Título revista: | Journal of Labelled Compounds and Radiopharmaceuticals |
| Título revista abreviado: | J. Label. Compd. Radiopharm. |
| ISSN: | 03624803 |
| Registro: | https://bibliotecadigital.exactas.uba.ar/collection/paper/document/paper_03624803_v23_n1_p109_Doller |
Referencias:
- Russo, C.A., Gros, E.G., (1981) Phytochemistry, 20, p. 1763
- Ghini, A.A., Burton, G., Gros, E.G., (1982) Phytochemistry, 21, p. 605
- Russo, C.A., Gros, E.G., (1982) Phytochemistry, 21, p. 609
- Russo, C.A., Burton, G., Gros, E.G., (1983) Phytochemistry, 22, p. 71
- Russo, C.A., Gros, E.G., (1983) Phytochemistry, 22, p. 1839
- Albright, I.D., (1974) J. Org. Chem., 39, p. 1977
- Klein, P.D., Knight, J.D., (1965) J. Am. Chem. Soc., 87, p. 2657
- Adam, G., Huang, H.Th., (1980) Tetrahedron Lett., 21, p. 1931
- Schreiber, K., Adam, G., (1961) Experientia, 17, p. 13
- Toldy, L., (1958) Acta. Chim. Acad. Sci Hung., 16, p. 403
- Bukovits, G.J., Daller, D., ; Uhle, F.C., (1961) J. Am. Chem. Soc., 83, p. 1460
Citas:
---------- APA ----------
Doller, D. & Gros, E.G. (1986) . Preparation of |2,4‐2H|‐ and |2,4‐3H|‐tomatidine. Journal of Labelled Compounds and Radiopharmaceuticals, 23(1), 109-112.http://dx.doi.org/10.1002/jlcr.2580230114
---------- CHICAGO ----------
Doller, D., Gros, E.G. "Preparation of |2,4‐2H|‐ and |2,4‐3H|‐tomatidine" . Journal of Labelled Compounds and Radiopharmaceuticals 23, no. 1 (1986) : 109-112.http://dx.doi.org/10.1002/jlcr.2580230114
---------- MLA ----------
Doller, D., Gros, E.G. "Preparation of |2,4‐2H|‐ and |2,4‐3H|‐tomatidine" . Journal of Labelled Compounds and Radiopharmaceuticals, vol. 23, no. 1, 1986, pp. 109-112.http://dx.doi.org/10.1002/jlcr.2580230114
---------- VANCOUVER ----------
Doller, D., Gros, E.G. Preparation of |2,4‐2H|‐ and |2,4‐3H|‐tomatidine. J. Label. Compd. Radiopharm. 1986;23(1):109-112.http://dx.doi.org/10.1002/jlcr.2580230114
