Artículo
Maier, M.S.; Seldes, A.M.; Gros, E.G. "Synthesis of |24‐14C|‐3β,14β,20ε‐trihydroxy‐23‐nor‐5β‐cholanoic acid" (1985) Journal of Labelled Compounds and Radiopharmaceuticals. 22(8):833-836
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Abstract:
The synthesis of |24‐14C|‐3β,14β,20ε‐trihydroxy‐23‐nor‐5β‐cholanoic acid was accomplished by Reformatsky reaction of ethyl |1‐14C|‐bromo acetate with 3β‐acetoxy‐14β‐hydroxy‐5β‐pregnan‐20‐one which was obtained from digitoxigenin. The final and intermediate products were characterized by spectroscopic (IR, 1H and 13C‐NMR, MS) methods. Copyright © 1985 John Wiley & Sons, Ltd.
Registro:
| Documento: | Artículo |
| Título: | Synthesis of |24‐14C|‐3β,14β,20ε‐trihydroxy‐23‐nor‐5β‐cholanoic acid |
| Autor: | Maier, M.S.; Seldes, A.M.; Gros, E.G. |
| Filiación: | Departamento de Quimica Orgànica Y Umymfor, Facultad de Ciencias Exactas Y Naturales, Universidad de Buenos Aires, Pabellón 2, Ciudad Universitaria, Buenos Aires, 1428, Argentina |
| Palabras clave: | Reformatsky reaction; Synthesis; |24‐14C|‐3β,14β,20ε‐Trihydroxy‐23‐nor‐5β‐cholanoic acid; radioisotope; 3beta,14beta,20 trihydroxy 23 norcholanic acid c 14; methodology; nonhuman; priority journal |
| Año: | 1985 |
| Volumen: | 22 |
| Número: | 8 |
| Página de inicio: | 833 |
| Página de fin: | 836 |
| DOI: | http://dx.doi.org/10.1002/jlcr.2580220810 |
| Título revista: | Journal of Labelled Compounds and Radiopharmaceuticals |
| Título revista abreviado: | J. Label. Compd. Radiopharm. |
| ISSN: | 03624803 |
| Registro: | https://bibliotecadigital.exactas.uba.ar/collection/paper/document/paper_03624803_v22_n8_p833_Maier |
Referencias:
- Galagovsky, L.R., Porto, A.M., Burton, G., Gros, E.G., (1984) Z. Naturforsch., 39 c, p. 38. , and previous papers cited therein
- Maier, M.S., Seldes, A.M., Gros, E.G., J. Lab. Compds Radiopharm. in press; Leete, E., Gregory, H., Gros, E.G., (1965) J. Am. Chem. Soc., 87, p. 3475
- Danieli, N., Mazur, Y., Sondheimer, F., (1962) J. Am. Chem. Soc., 84, p. 875
- Saret, L.H., US Patent 2912446; (1960) Chem. Abst., 54, p. 3527a
- Boots Pure Drug Co. Ltd., ‐ Fr. Patent 1513708; (1969) Chem. Abst., 71, p. 13284m
Citas:
---------- APA ----------
Maier, M.S., Seldes, A.M. & Gros, E.G. (1985) . Synthesis of |24‐14C|‐3β,14β,20ε‐trihydroxy‐23‐nor‐5β‐cholanoic acid. Journal of Labelled Compounds and Radiopharmaceuticals, 22(8), 833-836.http://dx.doi.org/10.1002/jlcr.2580220810
---------- CHICAGO ----------
Maier, M.S., Seldes, A.M., Gros, E.G. "Synthesis of |24‐14C|‐3β,14β,20ε‐trihydroxy‐23‐nor‐5β‐cholanoic acid" . Journal of Labelled Compounds and Radiopharmaceuticals 22, no. 8 (1985) : 833-836.http://dx.doi.org/10.1002/jlcr.2580220810
---------- MLA ----------
Maier, M.S., Seldes, A.M., Gros, E.G. "Synthesis of |24‐14C|‐3β,14β,20ε‐trihydroxy‐23‐nor‐5β‐cholanoic acid" . Journal of Labelled Compounds and Radiopharmaceuticals, vol. 22, no. 8, 1985, pp. 833-836.http://dx.doi.org/10.1002/jlcr.2580220810
---------- VANCOUVER ----------
Maier, M.S., Seldes, A.M., Gros, E.G. Synthesis of |24‐14C|‐3β,14β,20ε‐trihydroxy‐23‐nor‐5β‐cholanoic acid. J. Label. Compd. Radiopharm. 1985;22(8):833-836.http://dx.doi.org/10.1002/jlcr.2580220810
