Artículo
Baggio, R.; Garland, M.T.; Perec, M. "Synthesis and characterization of zinc(II) oxydiacetate (oda) complexes. Crystal structures of [{Zn(oda)·0.3H2O}n], [Zn(oda)(bipy)(H2O)]·2.5H2O and [Zn(oda)(phen)(H2O)]·1.5H2O (bipy = 2,2′-bipyridine, phen = 1,10-phenanthroline)" (1996) Journal of the Chemical Society - Dalton Transactions(13):2747-2753
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Abstract:
Three novel zinc(II) oxydiacetate (oda) compounds [{Zn(oda)·0.3H2O}n] 1, [Zn(oda)(bipy)(H2O)]·2.5H2O 2 (bipy = 2,2′-bipyridine) and [Zn(oda)(phen)(H2O)]·1.5H2O 3 (phen = 1,10-phenanthroline) have been synthesized and their structures determined by single-crystal X-ray diffraction methods. Compound 1 consists of polymeric sheets formed by ZnO5 units bridged by carboxylate groups in anti-syn conformation along the z axis; 2 and 3 are mononuclear with the zinc atoms in distorted octahedral ZnN2O4 co-ordination geometries. Thermal decomposition of the compounds under an oxygen atmosphere affords ZnO at ca. 500°C.
Registro:
| Documento: | Artículo |
| Título: | Synthesis and characterization of zinc(II) oxydiacetate (oda) complexes. Crystal structures of [{Zn(oda)·0.3H2O}n], [Zn(oda)(bipy)(H2O)]·2.5H2O and [Zn(oda)(phen)(H2O)]·1.5H2O (bipy = 2,2′-bipyridine, phen = 1,10-phenanthroline) |
| Autor: | Baggio, R.; Garland, M.T.; Perec, M. |
| Filiación: | División Física del Sólido, Departamento de Física, Comisión Nacional de Energía Atómica, Avda del Libertador 8250, 1429 Buenos Aires, Argentina Departamento de Física, Facultad de Ciencias Físicas y Matemáticas, Universidad de Chile, Av. Bl. Encalada 2008, Casilla 487-3, Santiago, Chile Depto. de Química Inorgánica, Analítica y Química Física, Instituto de Química Física de los Materialles, Medio Ambiente y Energía, Pabellón II, 1428, Buenos Aires, Argentina |
| Año: | 1996 |
| Número: | 13 |
| Página de inicio: | 2747 |
| Página de fin: | 2753 |
| DOI: | http://dx.doi.org/10.1039/DT9960002747 |
| Título revista: | Journal of the Chemical Society - Dalton Transactions |
| ISSN: | 03009246 |
| Registro: | https://bibliotecadigital.exactas.uba.ar/collection/paper/document/paper_03009246_v_n13_p2747_Baggio |
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Citas:
---------- APA ----------
Baggio, R., Garland, M.T. & Perec, M. (1996) . Synthesis and characterization of zinc(II) oxydiacetate (oda) complexes. Crystal structures of [{Zn(oda)·0.3H2O}n], [Zn(oda)(bipy)(H2O)]·2.5H2O and [Zn(oda)(phen)(H2O)]·1.5H2O (bipy = 2,2′-bipyridine, phen = 1,10-phenanthroline). Journal of the Chemical Society - Dalton Transactions(13), 2747-2753.http://dx.doi.org/10.1039/DT9960002747
---------- CHICAGO ----------
Baggio, R., Garland, M.T., Perec, M. "Synthesis and characterization of zinc(II) oxydiacetate (oda) complexes. Crystal structures of [{Zn(oda)·0.3H2O}n], [Zn(oda)(bipy)(H2O)]·2.5H2O and [Zn(oda)(phen)(H2O)]·1.5H2O (bipy = 2,2′-bipyridine, phen = 1,10-phenanthroline)" . Journal of the Chemical Society - Dalton Transactions, no. 13 (1996) : 2747-2753.http://dx.doi.org/10.1039/DT9960002747
---------- MLA ----------
Baggio, R., Garland, M.T., Perec, M. "Synthesis and characterization of zinc(II) oxydiacetate (oda) complexes. Crystal structures of [{Zn(oda)·0.3H2O}n], [Zn(oda)(bipy)(H2O)]·2.5H2O and [Zn(oda)(phen)(H2O)]·1.5H2O (bipy = 2,2′-bipyridine, phen = 1,10-phenanthroline)" . Journal of the Chemical Society - Dalton Transactions, no. 13, 1996, pp. 2747-2753.http://dx.doi.org/10.1039/DT9960002747
---------- VANCOUVER ----------
Baggio, R., Garland, M.T., Perec, M. Synthesis and characterization of zinc(II) oxydiacetate (oda) complexes. Crystal structures of [{Zn(oda)·0.3H2O}n], [Zn(oda)(bipy)(H2O)]·2.5H2O and [Zn(oda)(phen)(H2O)]·1.5H2O (bipy = 2,2′-bipyridine, phen = 1,10-phenanthroline). 1996(13):2747-2753.http://dx.doi.org/10.1039/DT9960002747
