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Abstract:

The influence of microstructure on the corrosion behavior of pulsed plasma nitrocarburized AISI H13 tool steel in NaCl 0.9 wt/V % solution is reported. The samples were prepared with different nitrocarburizing treatment times using a constant [CH4/H2 + N2] gaseous mixture by a DC pulsed plasma system. The microstructure of the nitrocarburized layers was analyzed by scanning electron microscopy (SEM), X-ray photoelectron spectroscopy (XPS) and X-ray diffraction. The corrosion behavior was evaluated by potentiodynamic polarization experiments. The nitrocarburizing process considerably improves the corrosion resistance of the material in a NaCl environment as compared to the untreated H13 steel. The modified surface layer mainly consisting of ε-Fe2-3(C,N) and γ′-Fe4N phases confers this outstanding behavior. The corrosion resistance dependence on specific nitrocarburizing processes is reported and the role of the surface porosity is discussed. © 2008 Elsevier B.V. All rights reserved.

Registro:

Documento: Artículo
Título:Influence of microstructure on the corrosion behavior of nitrocarburized AISI H13 tool steel obtained by pulsed DC plasma
Autor:Basso, R.L.O.; Candal, R.J.; Figueroa, C.A.; Wisnivesky, D.; Alvarez, F.
Filiación:Instituto de Física Gleb Wataghin, Unicamp, 13083-970 Campinas, São Paulo, Brazil
INQUIMAE-UBA, Ciudad Universitaria, Pabellon II, 1428 Buenos Aires, Argentina
Palabras clave:Plasma nitrocarburizing; Porosity analysis; Steel corrosion; Surface porosity; Tool steel; X-ray diffraction; Corrosion; Corrosion resistance; Corrosive effects; Diffraction; Industrial heating; Microstructure; Photoelectron spectroscopy; Plasmas; Porosity; Scanning electron microscopy; Sodium chloride; Steel; Steel corrosion; Surface treatment; Surfaces; X ray analysis; X ray diffraction; X ray diffraction analysis; X ray photoelectron spectroscopy; AISI H13; Corrosion behaviors; DC plasma; DC pulsed plasma; H13 steel; Nitrocarburizing; Nitrocarburizing process; Plasma nitrocarburizing; Polarization experiments; Porosity analysis; Surface layering; Surface porosity; Treatment times; X ray photoelectron spectroscopy (XPS); Tool steel
Año:2009
Volumen:203
Número:10-11
Página de inicio:1293
Página de fin:1297
DOI: http://dx.doi.org/10.1016/j.surfcoat.2008.10.006
Título revista:Surface and Coatings Technology
Título revista abreviado:Surf. Coat. Technol.
ISSN:02578972
Registro:https://bibliotecadigital.exactas.uba.ar/collection/paper/document/paper_02578972_v203_n10-11_p1293_Basso

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Citas:

---------- APA ----------
Basso, R.L.O., Candal, R.J., Figueroa, C.A., Wisnivesky, D. & Alvarez, F. (2009) . Influence of microstructure on the corrosion behavior of nitrocarburized AISI H13 tool steel obtained by pulsed DC plasma. Surface and Coatings Technology, 203(10-11), 1293-1297.
http://dx.doi.org/10.1016/j.surfcoat.2008.10.006
---------- CHICAGO ----------
Basso, R.L.O., Candal, R.J., Figueroa, C.A., Wisnivesky, D., Alvarez, F. "Influence of microstructure on the corrosion behavior of nitrocarburized AISI H13 tool steel obtained by pulsed DC plasma" . Surface and Coatings Technology 203, no. 10-11 (2009) : 1293-1297.
http://dx.doi.org/10.1016/j.surfcoat.2008.10.006
---------- MLA ----------
Basso, R.L.O., Candal, R.J., Figueroa, C.A., Wisnivesky, D., Alvarez, F. "Influence of microstructure on the corrosion behavior of nitrocarburized AISI H13 tool steel obtained by pulsed DC plasma" . Surface and Coatings Technology, vol. 203, no. 10-11, 2009, pp. 1293-1297.
http://dx.doi.org/10.1016/j.surfcoat.2008.10.006
---------- VANCOUVER ----------
Basso, R.L.O., Candal, R.J., Figueroa, C.A., Wisnivesky, D., Alvarez, F. Influence of microstructure on the corrosion behavior of nitrocarburized AISI H13 tool steel obtained by pulsed DC plasma. Surf. Coat. Technol. 2009;203(10-11):1293-1297.
http://dx.doi.org/10.1016/j.surfcoat.2008.10.006