Abstract:
An isotopic dilution method for the determination of traces of molybdenum has been developed. The method consists of the complexation Mo(V)-SCN with substoichiometric quantities of crystal violet, and its subsequent extraction into chloroform. This procedure was successfully tested for the determination of molybdenum in the range of 0.5 to 20 μg. © 1995 Akadémiai Kiadó.
Registro:
Documento: |
Artículo
|
Título: | Substoichiometric radiochemical determination of molybdenum with crystal violet |
Autor: | Rosenbusch, M.; Di Risio, C.; Marques, R. |
Filiación: | Departmento de Química Inorgánica, Analítica y Química Física, Facultad de Ciencias Exactas y Naturales, Universidad de Buenos Aires, Ciudad Universitaria, Pab. II, Buenos Aires, 1428, Argentina
|
Palabras clave: | crystal violet; molybdenum; article; calorimetry; isotope dilution assay; methodology; quantitative assay |
Año: | 1995
|
Volumen: | 199
|
Número: | 4
|
Página de inicio: | 333
|
Página de fin: | 338
|
DOI: |
http://dx.doi.org/10.1007/BF02162460 |
Título revista: | Journal of Radioanalytical and Nuclear Chemistry Letters
|
Título revista abreviado: | J. Radioanal. Nucl. Chem.
|
ISSN: | 02365731
|
CODEN: | JRNCD
|
Registro: | https://bibliotecadigital.exactas.uba.ar/collection/paper/document/paper_02365731_v199_n4_p333_Rosenbusch |
Referencias:
- Dee, Snell, P, (1979) Photometric and Fluorimetric Methods of Analysis, Part 2, Chapter 28, p. 1295. , Foster Dee Snell, John Wiley & Sons, NY
- Nadkarni, R.A., Haldar, B.C., (1972) Radiochem. Radioanal. Lett., 10, p. 183
Citas:
---------- APA ----------
Rosenbusch, M., Di Risio, C. & Marques, R.
(1995)
. Substoichiometric radiochemical determination of molybdenum with crystal violet. Journal of Radioanalytical and Nuclear Chemistry Letters, 199(4), 333-338.
http://dx.doi.org/10.1007/BF02162460---------- CHICAGO ----------
Rosenbusch, M., Di Risio, C., Marques, R.
"Substoichiometric radiochemical determination of molybdenum with crystal violet"
. Journal of Radioanalytical and Nuclear Chemistry Letters 199, no. 4
(1995) : 333-338.
http://dx.doi.org/10.1007/BF02162460---------- MLA ----------
Rosenbusch, M., Di Risio, C., Marques, R.
"Substoichiometric radiochemical determination of molybdenum with crystal violet"
. Journal of Radioanalytical and Nuclear Chemistry Letters, vol. 199, no. 4, 1995, pp. 333-338.
http://dx.doi.org/10.1007/BF02162460---------- VANCOUVER ----------
Rosenbusch, M., Di Risio, C., Marques, R. Substoichiometric radiochemical determination of molybdenum with crystal violet. J. Radioanal. Nucl. Chem. 1995;199(4):333-338.
http://dx.doi.org/10.1007/BF02162460