Artículo
D'Alessandro, C.; Giacopello, S.; Seldes, A.M.; Deluca, M.E. "Reduction of a Δ4-Steroid with Diborane" (1995) Synthetic Communications. 25(18):2703-2708
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Abstract:
Reported here is a boron process equivalent to stereoselective olefin reduction and concomitant protecting group cleavage. © 1995, Taylor & Francis Group, LLC. All rights reserved.
Registro:
| Documento: | Artículo |
| Título: | Reduction of a Δ4-Steroid with Diborane |
| Autor: | D'Alessandro, C.; Giacopello, S.; Seldes, A.M.; Deluca, M.E. |
| Filiación: | Departamento de Química Orgánica, Facultad de Ciencias Exactas y Naturales, Universidad de Buenos Aires, (1428), Buenos Aires, Argentina |
| Palabras clave: | 5β-steroids; boron rearrangement; molecular mechanics; synthesis; cholesterol derivative; article; drug synthesis; methodology; nuclear magnetic resonance; reduction; stereochemistry |
| Año: | 1995 |
| Volumen: | 25 |
| Número: | 18 |
| Página de inicio: | 2703 |
| Página de fin: | 2708 |
| DOI: | http://dx.doi.org/10.1080/00397919508011818 |
| Título revista: | Synthetic Communications |
| Título revista abreviado: | Synth. Commun. |
| ISSN: | 00397911 |
| Registro: | https://bibliotecadigital.exactas.uba.ar/collection/paper/document/paper_00397911_v25_n18_p2703_DAlessandro |
Referencias:
- Snyder, B.W., Winneker, R.C., Batzold, F.H., (1989) J. Steroid Biochem., 33, p. 1127
- Christiansen, R.G., Bell, M.R., D'Ambra, T.E., Mallamo, J.P., Herrmann, J.L., Ackerman, J.H., Opalka, C.J., Schane, H.P., (1990) J. Med. Chem., 33 (8), p. 2094
- Blunt, J.W., Stothers, J.B., (1977) Org. Magn. Reson., 9 (8), p. 439
- Dart, M.C., Henbest, H.B., (1960) J. Chem. Soc, p. 3563
- Fried, J., Edwards, J.A., (1972), 1. , Eds.; Van Nostrand Reinhold: New York, Chapter 3; Ravasio, N., Rossi, M., (1991) J. Org. Chem., 56, p. 4329
- Allinger, N.L., (1977), The force field used in PCMODEL is called MMX and is derived from the MM2(QCPE-395) force field of, with the pi-VESCF routines taken from MMP1(QCPE-318), also by N.L. Allinger; Bryson, T.A., Akers, J.A., Ergle, J.D., (1991) Synlett, p. 499
Citas:
---------- APA ----------
D'Alessandro, C., Giacopello, S., Seldes, A.M. & Deluca, M.E. (1995) . Reduction of a Δ4-Steroid with Diborane. Synthetic Communications, 25(18), 2703-2708.http://dx.doi.org/10.1080/00397919508011818
---------- CHICAGO ----------
D'Alessandro, C., Giacopello, S., Seldes, A.M., Deluca, M.E. "Reduction of a Δ4-Steroid with Diborane" . Synthetic Communications 25, no. 18 (1995) : 2703-2708.http://dx.doi.org/10.1080/00397919508011818
---------- MLA ----------
D'Alessandro, C., Giacopello, S., Seldes, A.M., Deluca, M.E. "Reduction of a Δ4-Steroid with Diborane" . Synthetic Communications, vol. 25, no. 18, 1995, pp. 2703-2708.http://dx.doi.org/10.1080/00397919508011818
---------- VANCOUVER ----------
D'Alessandro, C., Giacopello, S., Seldes, A.M., Deluca, M.E. Reduction of a Δ4-Steroid with Diborane. Synth. Commun. 1995;25(18):2703-2708.http://dx.doi.org/10.1080/00397919508011818
