Artículo
Porto, A.M.; Gros, E.G. "Synthesis of cholesterol‐20‐14C" (1970) Journal of Labelled Compounds. 6(4):369-372
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Abstract:
Cholesterol‐20‐14C was synthesized in four steps from pregnenolone‐20‐14C. The labelled intermediates were proven to be cholest‐5‐ene‐3β, 20α‐diol acetate‐3, cholesta‐5, 20 (22)‐diene‐3β‐ol acetate, and cholesterol acetate by 1H‐n.m.r. spectroscopical analysis. Cholesterol‐20‐14C was obtained with a radiochemical purity exceeding 99%. Copyright © 1970 John Wiley & Sons, Ltd.
Registro:
| Documento: | Artículo |
| Título: | Synthesis of cholesterol‐20‐14C |
| Autor: | Porto, A.M.; Gros, E.G. |
| Filiación: | Departamento de Química Orgánica, Facultad de Ciencias Exactas y Naturales, Universidad de Buenos Aires, Perü 222, Buenos Aires, Argentina |
| Año: | 1970 |
| Volumen: | 6 |
| Número: | 4 |
| Página de inicio: | 369 |
| Página de fin: | 372 |
| DOI: | http://dx.doi.org/10.1002/jlcr.2590060410 |
| Título revista: | Journal of Labelled Compounds |
| Título revista abreviado: | J. Label. Compd. Radiopharm. |
| ISSN: | 00222135 |
| Registro: | https://bibliotecadigital.exactas.uba.ar/collection/paper/document/paper_00222135_v6_n4_p369_Porto |
Referencias:
- Porto, A.M., Gros, E.G., (1970) Experientia, 26, p. 11
- Porto, A.M., Gros, E.G., Synthesis of PREGN-5-en-3β-o1-20-one-20-14C (1968) Journal of Labelled Compounds, 4, p. 276
- Sabetay, S., Bléger, J., (1930) Bull. Soc. Chim. France, 47, p. 885
- Petrow, V., Stuart‐Webb, I.A., J. Chem. Soc., 1956, p. 4675
- Bergman, E.D., Rabinovitz, M., Levinson, Z.H., The Synthesis and Biological Availability of Some Lower Homologs of Cholesterol (1959) Journal of the American Chemical Society, 81, p. 1239
- Mijares, A., Cargill, D.I., Glasel, J.A., Lieberman, S., (1967) J. Org. Chem., 32, p. 810
- Koechlin, B., Reichstein, T., (1944) Helvetica Chimica Acta, 27, p. 549
- Sondheimer, F., Mechoulam, R., (1958) J. Amer. Chem. Soc., 80, p. 3087
- Hershberg, E.B., Oliveto, E.P., Gerold, C., Johnson, L., (1951) J. Amer. Chem. Soc., 73, p. 5073. , see also ref. 5
Citas:
---------- APA ----------
Porto, A.M. & Gros, E.G. (1970) . Synthesis of cholesterol‐20‐14C. Journal of Labelled Compounds, 6(4), 369-372.http://dx.doi.org/10.1002/jlcr.2590060410
---------- CHICAGO ----------
Porto, A.M., Gros, E.G. "Synthesis of cholesterol‐20‐14C" . Journal of Labelled Compounds 6, no. 4 (1970) : 369-372.http://dx.doi.org/10.1002/jlcr.2590060410
---------- MLA ----------
Porto, A.M., Gros, E.G. "Synthesis of cholesterol‐20‐14C" . Journal of Labelled Compounds, vol. 6, no. 4, 1970, pp. 369-372.http://dx.doi.org/10.1002/jlcr.2590060410
---------- VANCOUVER ----------
Porto, A.M., Gros, E.G. Synthesis of cholesterol‐20‐14C. J. Label. Compd. Radiopharm. 1970;6(4):369-372.http://dx.doi.org/10.1002/jlcr.2590060410
