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Abstract:

We report herein the synthesis of new synthons obtained by reductive opening of 3-glycosyl-5-substituted-2-isoxazolines. Different cleavage products have been obtained depending on the substituents (aliphatic or aromatic) in position five of the heterocycle ring. The new compounds are characterized physically and spectroscopically.

Registro:

Documento: Artículo
Título:Characterization and identification of cleavage products of 3-glycosyl-5-substituted-2-isoxazoline
Autor:Gelabert, L.I.; Fascio, M.L.; D'Accorso, N.B.
Filiación:CIHIDECAR, Departamento de Quimica Organica, Universidad de Buenos Aires, Ciudad Universitaria, Buenos Aires, Argentina
Palabras clave:aliphatic compound; aromatic compound; chemical compound; heterocyclic compound; isoxazoline derivative; article; carbon nuclear magnetic resonance; physical chemistry; protein analysis; protein degradation; proton nuclear magnetic resonance; spectroscopy
Año:2003
Volumen:40
Número:2
Página de inicio:341
Página de fin:344
DOI: http://dx.doi.org/10.1002/jhet.5570400223
Título revista:Journal of Heterocyclic Chemistry
Título revista abreviado:J. Heterocycl. Chem.
ISSN:0022152X
CODEN:JHTCA
Registro:https://bibliotecadigital.exactas.uba.ar/collection/paper/document/paper_0022152X_v40_n2_p341_Gelabert

Referencias:

  • Kwon, T., Heiman, A.S., Oriaku, E.T., Yoon, K., Lee, H.J., (1995) J. Med. Chem., 38, p. 1048
  • Gordaliza, M., Faircloth, G.T., Castro, M.A., Miguel del Corral, J.M., Lopez-Vazquez, M.L., San Feliciano, A., (1996) J. Med. Chem., 39, p. 2865
  • Kozikowski, A.P., (1984) Acc. Chem. Res., 17, p. 410
  • Fascio, M.L., D'Accorso, N.B., (1996) J. Heterocyclic Chem., 33, p. 1573
  • Fascio, M.L., Montesano, V.J., D'Accorso, N.B., (1998) J. Heterocyclic Chem., 35, p. 103
  • D'Accorso, N., Fascio, M., Arabehety, C.G., Seldes, A.M., (1999) J. Mass Spectrom., 34, p. 915
  • Auricchio, S., Ricca, A., (1987) Tetrahedron, 43, p. 3983

Citas:

---------- APA ----------
Gelabert, L.I., Fascio, M.L. & D'Accorso, N.B. (2003) . Characterization and identification of cleavage products of 3-glycosyl-5-substituted-2-isoxazoline. Journal of Heterocyclic Chemistry, 40(2), 341-344.
http://dx.doi.org/10.1002/jhet.5570400223
---------- CHICAGO ----------
Gelabert, L.I., Fascio, M.L., D'Accorso, N.B. "Characterization and identification of cleavage products of 3-glycosyl-5-substituted-2-isoxazoline" . Journal of Heterocyclic Chemistry 40, no. 2 (2003) : 341-344.
http://dx.doi.org/10.1002/jhet.5570400223
---------- MLA ----------
Gelabert, L.I., Fascio, M.L., D'Accorso, N.B. "Characterization and identification of cleavage products of 3-glycosyl-5-substituted-2-isoxazoline" . Journal of Heterocyclic Chemistry, vol. 40, no. 2, 2003, pp. 341-344.
http://dx.doi.org/10.1002/jhet.5570400223
---------- VANCOUVER ----------
Gelabert, L.I., Fascio, M.L., D'Accorso, N.B. Characterization and identification of cleavage products of 3-glycosyl-5-substituted-2-isoxazoline. J. Heterocycl. Chem. 2003;40(2):341-344.
http://dx.doi.org/10.1002/jhet.5570400223