Abstract:
As an aid to the structural determination of naturally methylated galactans, the separation and identification by capillary gas chromatography and the mass spectral features of ethylated galactoses as their aldononitrile and alditol acetate derivatives are presented and compared with those of their methylated counterparts. Data for some ethylated mono-O-methylgalactose derivatives are also included. © 1994.
Registro:
Documento: |
Artículo
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Título: | Separation and identification of partially ethylated galactoses as their acetylated aldononitriles and alditols by capillary gas chromatography and mass spectrometry |
Autor: | Cases, M.R.; Stortz, C.A.; Cerezo, A.S. |
Filiación: | Departamento de Química Orgánica, Facultad de Ciencias Exactas y Naturales, UBA, Ciudad Universitaria, 1428 Buenos Aires, Argentina
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Palabras clave: | galactan; article; carbohydrate analysis; gas liquid chromatography; mass spectrometry; priority journal |
Año: | 1994
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Volumen: | 662
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Número: | 2
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Página de inicio: | 293
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Página de fin: | 299
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DOI: |
http://dx.doi.org/10.1016/0021-9673(94)80517-2 |
Título revista: | Journal of Chromatography A
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Título revista abreviado: | J. Chromatogr. A
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ISSN: | 00219673
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CODEN: | JCRAE
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CAS: | galactan, 39300-87-3, 9037-55-2
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Registro: | https://bibliotecadigital.exactas.uba.ar/collection/paper/document/paper_00219673_v662_n2_p293_Cases |
Referencias:
- Aspinall, (1982) The Polysaccharides, 1, p. 36. , G.O. Aspinall, Academic Press, Orlando
- Björndal, Hellerqvist, Lindberg, Svensson, Gas-Liquid Chromatography and Mass Spectrometry in Methylation Analysis of Polysaccharides (1970) Angewandte Chemie International Edition in English, 9, p. 610
- Stortz, Matulewicz, Cerezo, (1982) Carbohydr. Res., 111, p. 31
- Tanner, Morrison, (1984) J. Chromatogr., 299, p. 252
- Lindberg, Lönngren, Nimmich, (1972) Acta Chem. Scand., 26, p. 2231
- Saier, Ballou, (1968) J. Biol. Chem., 243, p. 992
- Sweet, Albersheim, Shapiro, (1975) Carbohydr. Res., 40, p. 199
- Sweet, Shapiro, Albersheim, (1974) Biomed. Mass Spectrom., 1, p. 263
- Painter, (1982) The Polysaccharides, 2, p. 195. , G.O. Aspinall, Academic Press, Orlando
- Cases, Stortz, Cerezo, (1992) Phytochemistry, 31, p. 3897
- Shea, Carpita, (1988) J. Chromatogr., 445, p. 424
- Stortz, Cerezo, (1993) Carbohydr. Res., 242, p. 217
- Stevenson, Furneaux, (1991) Carbohydr. Res., 210, p. 277
- Hunt, (1920) J. Chem. Soc., 117, p. 1592
- M.R. Cases, C.A. Stortz, A.S. Cerezo, Int. J. Biol. Macromol., submitted for publication; Klok, Cox, de Leeuw, Schenck, (1982) J. Chromatogr., 253, p. 55
Citas:
---------- APA ----------
Cases, M.R., Stortz, C.A. & Cerezo, A.S.
(1994)
. Separation and identification of partially ethylated galactoses as their acetylated aldononitriles and alditols by capillary gas chromatography and mass spectrometry. Journal of Chromatography A, 662(2), 293-299.
http://dx.doi.org/10.1016/0021-9673(94)80517-2---------- CHICAGO ----------
Cases, M.R., Stortz, C.A., Cerezo, A.S.
"Separation and identification of partially ethylated galactoses as their acetylated aldononitriles and alditols by capillary gas chromatography and mass spectrometry"
. Journal of Chromatography A 662, no. 2
(1994) : 293-299.
http://dx.doi.org/10.1016/0021-9673(94)80517-2---------- MLA ----------
Cases, M.R., Stortz, C.A., Cerezo, A.S.
"Separation and identification of partially ethylated galactoses as their acetylated aldononitriles and alditols by capillary gas chromatography and mass spectrometry"
. Journal of Chromatography A, vol. 662, no. 2, 1994, pp. 293-299.
http://dx.doi.org/10.1016/0021-9673(94)80517-2---------- VANCOUVER ----------
Cases, M.R., Stortz, C.A., Cerezo, A.S. Separation and identification of partially ethylated galactoses as their acetylated aldononitriles and alditols by capillary gas chromatography and mass spectrometry. J. Chromatogr. A. 1994;662(2):293-299.
http://dx.doi.org/10.1016/0021-9673(94)80517-2