Artículo
Baggio, R.; Garland, M.T.; Leyva, G.; Perec, M.; Polla, G. "Synthesis and structure of two polymeric barium-oxydiacetates: [Ba(oda)·H2O]n and [Ba(Hoda)2] n (H2oda: Oxydiacetic acid)" (2004) Inorganica Chimica Acta. 357(7):2185-2190
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Abstract:
The reaction of barium carbonate or hydroxide with oxydiacetic acid leads to the self-assembly of two barium oxydiacetate polymers in good yield: [Ba(oda)·H2O]n (1) and [Ba(Hoda)2] n (2). The products have been characterized by elemental analysis, IR, TGA and single crystal X-ray diffraction studies. The central barium atom in each mononuclear fragment is nine-coordinate in 1 and 10-coordinate in 2. These fragments are bridged by carboxylato groups in anti-anti conformation and through H-bonds bonding interactions forming complex 3D networks. © 2003 Elsevier B.V. All rights reserved.
Registro:
| Documento: | Artículo |
| Título: | Synthesis and structure of two polymeric barium-oxydiacetates: [Ba(oda)·H2O]n and [Ba(Hoda)2] n (H2oda: Oxydiacetic acid) |
| Autor: | Baggio, R.; Garland, M.T.; Leyva, G.; Perec, M.; Polla, G. |
| Filiación: | Departamento de Física, Comn. Nac. de Ener. Atómica, Avda del Libertador 8250, 1429 Buenos Aires, Argentina Departamento de Física, Fac. de Cie. Fis. Y Matemat., Universidad de Chile, Avda. B. E. 2008, Casilla 487-3, Santiago, Chile Depto. de Quim. Inorgánica, Analítica Y Quim. Fis., Pabellón II 1428, Buenos Aires, Argentina |
| Palabras clave: | Barium complexes; Carboxylates; Crystal Structures; Hydrogen bonds; acetoacetic acid derivative; barium derivative; article; atom; conformation; crystal structure; hydrogen bond; infrared spectroscopy; molecular interaction; structure analysis; X ray diffraction |
| Año: | 2004 |
| Volumen: | 357 |
| Número: | 7 |
| Página de inicio: | 2185 |
| Página de fin: | 2190 |
| DOI: | http://dx.doi.org/10.1016/j.ica.2003.11.003 |
| Título revista: | Inorganica Chimica Acta |
| Título revista abreviado: | Inorg. Chim. Acta |
| ISSN: | 00201693 |
| CODEN: | ICHAA |
| Registro: | https://bibliotecadigital.exactas.uba.ar/collection/paper/document/paper_00201693_v357_n7_p2185_Baggio |
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Citas:
---------- APA ----------
Baggio, R., Garland, M.T., Leyva, G., Perec, M. & Polla, G. (2004) . Synthesis and structure of two polymeric barium-oxydiacetates: [Ba(oda)·H2O]n and [Ba(Hoda)2] n (H2oda: Oxydiacetic acid). Inorganica Chimica Acta, 357(7), 2185-2190.http://dx.doi.org/10.1016/j.ica.2003.11.003
---------- CHICAGO ----------
Baggio, R., Garland, M.T., Leyva, G., Perec, M., Polla, G. "Synthesis and structure of two polymeric barium-oxydiacetates: [Ba(oda)·H2O]n and [Ba(Hoda)2] n (H2oda: Oxydiacetic acid)" . Inorganica Chimica Acta 357, no. 7 (2004) : 2185-2190.http://dx.doi.org/10.1016/j.ica.2003.11.003
---------- MLA ----------
Baggio, R., Garland, M.T., Leyva, G., Perec, M., Polla, G. "Synthesis and structure of two polymeric barium-oxydiacetates: [Ba(oda)·H2O]n and [Ba(Hoda)2] n (H2oda: Oxydiacetic acid)" . Inorganica Chimica Acta, vol. 357, no. 7, 2004, pp. 2185-2190.http://dx.doi.org/10.1016/j.ica.2003.11.003
---------- VANCOUVER ----------
Baggio, R., Garland, M.T., Leyva, G., Perec, M., Polla, G. Synthesis and structure of two polymeric barium-oxydiacetates: [Ba(oda)·H2O]n and [Ba(Hoda)2] n (H2oda: Oxydiacetic acid). Inorg. Chim. Acta. 2004;357(7):2185-2190.http://dx.doi.org/10.1016/j.ica.2003.11.003
