Artículo

Urrutia, G.; Bonelli, P.; Cassanello, M.C.; Cukierman, A.L. "On dynamic liquid holdup determination by the drainage method" (1996) Chemical Engineering Science. 51(15):3721-3726
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Abstract:

A careful examination of the liquid drainage in packed-bed reactors using liquid superficial velocities characteristic of trickle flow regime and no gas velocity is both experimentally and theoretically carried out. True free-flowing or dynamic liquid holdups are determined in two different reactors packed with porous and nonporous particles employing several liquids. Dynamic liquid holdups are shown to be higher than those determined directly from total liquid drained volumes, which are usually reported when the drainage method is applied. It is found that a model of laminar liquid films properly addresses the influence of liquid superficial velocities and of liquid viscosity on the dynamic liquid holdup within the experimental conditions studied. A simple quantitative phenomenological model to describe the drainage kinetics is developed and is independently verified from experimental data. Satisfactory agreement is found for all the examined conditions.

Registro:

Documento: Artículo
Título:On dynamic liquid holdup determination by the drainage method
Autor:Urrutia, G.; Bonelli, P.; Cassanello, M.C.; Cukierman, A.L.
Filiación:Comision Nac. de Energia Atomica, Gerencia de Investigaciones, Av. Libertador 8250, 1429 Buenos Aires, Argentina
Fac. de Ciencias Exactas y Naturales, Ciudad Universitaria, Universidad de Buenos Aires, 1428 Buenos Aires, Argentina
Palabras clave:drainage; hold-up; packed beds; Fluid dynamics; Laminar flow; Mathematical models; Packed beds; Particles (particulate matter); Viscosity of liquids; Dynamic liquid holdup; Liquid superficial velocities; Trickle flow; Chemical reactors
Año:1996
Volumen:51
Número:15
Página de inicio:3721
Página de fin:3726
DOI: http://dx.doi.org/10.1016/0009-2509(96)00017-6
Título revista:Chemical Engineering Science
Título revista abreviado:CHEM. ENG. SCI.
ISSN:00092509
CODEN:CESCA
Registro:https://bibliotecadigital.exactas.uba.ar/collection/paper/document/paper_00092509_v51_n15_p3721_Urrutia

Referencias:

  • Berner, G.G., Kalis, G.A.J., A new method to predict hold-up and pressure drop in packed columns (1978) Trans. Instn Chem. Engrs, 56, pp. 200-204
  • Buchanan, J.E., Holdup in irrigated ring-packed towers below the loading point (1967) Ind. Engng Chem. Fundam., 6, pp. 400-407
  • Cassanello, M.C., Martínez, O.M., Cukierman, A.L., Effect of the liquid axial dispersion on the behavior of fixed bed three phase reactors (1992) Chem. Engng Sci., 47, pp. 3331-3338
  • Clements, L.D., Schmidt, P.C., Dynamic liquid holdup in two phase downflow in packed beds: Air-silicone oil system (1980) A.I.Ch.E. J., 26, pp. 317-319
  • Davidson, J.F., The hold-up and liquid film coefficient of packed towers. Part II: Statistical models of the random packing (1959) Trans. Instn Chem. Engrs, 37, pp. 131-136
  • Hasokowati, W., Hudgins, R.R., Silveston, P.L., Loading, draining and hold-up in periodically operated trickle-bed reactors (1994) Can. J. Chem. Engng, 72, pp. 405-410
  • Hofmann, H., (1986) Multiphase Chemical Reactors: Theory, Design, Scale-up, , Edited by Gianetto, A. and Silveston, P. L., Chap. 8. Hemisphere, Washington, DC
  • Holub, R.A., Dudukovic, M.P., Ramachandran, P.A., Pressure drop, liquid holdup, and flow regime transition in trickle flow (1993) A.I.Ch.E. J., 39, pp. 302-321
  • Kantzas, A., Computations of holdups in fluidized and trickle-beds by computer-assisted tomography (1994) A.I.Ch.E. J., 40, pp. 1254-1267
  • Martinez, O.M., Cassanello, M.C., Cukierman, A.L., Three-phase fixed bed catalytic reactors: Application to hydrotreatment processes (1994) Trends in Chemical Engineering, , Council of Scientific Research Integration, India
  • Nenninger E., Jr., Storrow, J.A., Drainage of packed beds in gravitational and centrifugal-force fields (1958) A.I.Ch.E. J., 4, pp. 305-316
  • Sáez, A.E., Yépez, M.M., Cabrera, C., Soria, E.M., Static liquid holdup in packed beds of spherical particles (1991) A.I.Ch.E. J., 37, pp. 1733-1736
  • Schubert, C.N., Lindner, J.R., Kelly, R.M., Experimental methods for measuring static liquid holdup in packed columns (1986) A.I.Ch.E. J., 32, pp. 1920-1923
  • Shirato, M., Murase, T., Mori, H., Mizuno, Y., Ogura, T., Nakai, E., Gravitational drainage of a granular packed bed (1981) Int. Chem. Engng, 21, pp. 294-302
  • Tukac, V., Hanika, J., Influence of catalyst particles orientation on the pressure drop and the liquid dispersion in the trickle-bed reactor (1992) Chem. Engng Sci., 47, pp. 2227-2232
  • Wakeman, R.J., Vince, A., Kinetics of gravity drainage from porous media (1986) Trans. Instn Chem. Engrs Dev., 64, pp. 94-103
  • Wild, G., Larachi, F., Laurent, A., The hydrodynamic characteristics of cocurrent downflow and cocurrent upflow gas-liquid-solid catalytic fixed bed reactors: The effect of pressure (1991) Rev. de L'Institut Francais du Petrole, 46, pp. 467-490
  • Yang, X.L., Wild, G., Euzen, J.P., Etude de la rétention liquide dans les réacteurs à lit fixe avec écoulement ascendant de gaz et de liquide (1989) Entropie, 150, pp. 17-28

Citas:

---------- APA ----------
Urrutia, G., Bonelli, P., Cassanello, M.C. & Cukierman, A.L. (1996) . On dynamic liquid holdup determination by the drainage method. Chemical Engineering Science, 51(15), 3721-3726.
http://dx.doi.org/10.1016/0009-2509(96)00017-6
---------- CHICAGO ----------
Urrutia, G., Bonelli, P., Cassanello, M.C., Cukierman, A.L. "On dynamic liquid holdup determination by the drainage method" . Chemical Engineering Science 51, no. 15 (1996) : 3721-3726.
http://dx.doi.org/10.1016/0009-2509(96)00017-6
---------- MLA ----------
Urrutia, G., Bonelli, P., Cassanello, M.C., Cukierman, A.L. "On dynamic liquid holdup determination by the drainage method" . Chemical Engineering Science, vol. 51, no. 15, 1996, pp. 3721-3726.
http://dx.doi.org/10.1016/0009-2509(96)00017-6
---------- VANCOUVER ----------
Urrutia, G., Bonelli, P., Cassanello, M.C., Cukierman, A.L. On dynamic liquid holdup determination by the drainage method. CHEM. ENG. SCI. 1996;51(15):3721-3726.
http://dx.doi.org/10.1016/0009-2509(96)00017-6